Basics of Analytical Chemistry and Chemical Equilibria 2e By Brian Tissue (informative)
Free download Basics of Analytical Chemistry and Chemical Equilibria 2e By Brian Tissue
2nd Edition
Authors of: Basics of Analytical Chemistry and Chemical Equilibria 2e By Brian Tissue
Brian M. Tissue
Table of Contents in Basics of Analytical Chemistry and Chemical Equilibria 2e By Brian Tissue
Preface
About the Companion Website
Part I: Quantitative Analysis Using Reactions That Go to “Completion”
Chapter 1: Making Measurements
1. Introduction
An overview of measurement techniques in quantitative analysis.
2. GLP and Other Important Acronyms
Explanation of Good Laboratory Practice and key acronyms used in the field.
3. Precision and Random Error
Discusses the importance of precision in measurements and how to manage random errors.
4. Discarding a Suspected Outlier
Guidelines for identifying and handling outliers in data.
5. Calibration
Techniques and importance of calibrating instruments and measurements.
6. Maintaining Accurate Results
Methods for ensuring accuracy in quantitative analysis.
Practice Exercises
Exercises to reinforce concepts and techniques from this chapter.
Chapter 2: Sample Preparation, Extractions, and Chromatography
1. Sampling and Control Samples
The process of obtaining representative samples and using control samples.
2. Sample Preparation
Steps involved in preparing samples for analysis.
3. Solvents and Solutions
Basics of using solvents and preparing solutions.
4. Introduction to Solubility
Fundamentals of solubility and its significance in extractions.
5. Extraction and Partitioning Theory
Theories behind extraction methods and partitioning.
6. Introduction to Stationary Phases
Understanding stationary phases in chromatography.
7. Solid-Phase Extraction (SPE)
Techniques and applications of SPE.
8. Column Chromatography
Principles and practices of column chromatography.
Practice Exercises
Exercises to practice skills learned in sample preparation and chromatography.
Chapter 3: Classical Methods
1. Introduction
Overview of classical methods in quantitative analysis.
2. Review of Chemical Reactions
Key chemical reactions used in classical methods.
3. Reactions in Aqueous Solution
Behavior and analysis of reactions occurring in aqueous solutions.
4. Gravimetry
Methods of quantitative analysis based on mass measurement.
5. Titration
Techniques and principles of titration.
6. Titration Curves
Interpretation and use of titration curves.
7. Coulometry
Electrochemical methods for measuring the amount of substance.
Practice Exercises
Exercises focusing on classical methods and their applications.
Chapter 4: Molecular Spectroscopy
1. Introduction
Basics of molecular spectroscopy.
2. Properties of EM Radiation
Characteristics of electromagnetic radiation relevant to spectroscopy.
3. Electromagnetic Spectrum
Overview of the EM spectrum and its segments.
4. Spectroscopic Transitions
Types of transitions observed in spectroscopy.
5. UV/Vis Absorption Spectroscopy
Principles and applications of UV/Vis absorption spectroscopy.
6. UV/Vis Instrumentation
Equipment used in UV/Vis spectroscopy.
7. Beer–Lambert Law
Explanation and use of the Beer–Lambert law in quantitative analysis.
8. Molecular Fluorescence
Principles and applications of fluorescence in molecular spectroscopy.
Practice Exercises
Exercises to apply concepts of molecular spectroscopy.
Part II: Reactions That Do Not Go to “Completion.” Equilibria in Aqueous Solutions
Chapter 5: Acid–Base Equilibria and Activity
1. Acids and Bases
Definitions and properties of acids and bases.
2. Weak Acids and Weak Bases
Behavior of weak acids and bases in equilibrium.
3. Water and Kw
The ionization of water and its equilibrium constant.
4. Acid Strength
Factors influencing the strength of acids.
5. The Concept of Activity
Understanding activity in the context of equilibria.
6. Acid–Base Equilibrium Calculations
Methods for calculating acid-base equilibria.
Practice Exercises
Exercises to reinforce understanding of acid-base equilibria.
Chapter 6: Buffer Solutions and Polyprotic Acids
1. Buffer Solutions
Preparation and use of buffer solutions.
2. Alpha Fraction Plots
Use of alpha fraction plots in understanding buffer systems.
3. Weak Acid Titration Curve
Interpretation of titration curves for weak acids.
4. Polyprotic Acids
Behavior and analysis of polyprotic acids.
Practice Exercises
Exercises on buffer solutions and polyprotic acids.
Chapter 7: Metal–Ligand Complexation
1. Complex Terminology
Key terms in metal-ligand complexation.
2. Complex Equilibria
Equilibrium considerations in complex formation.
3. Competing Equilibria
Impact of competing equilibria on complexation.
4. Stepwise Complexation
Stepwise formation and analysis of complexes.
5. Immunoassays
Use of immunoassays in complexation studies.
Practice Exercises
Exercises on metal-ligand complexation principles.
Chapter 8: Precipitation Equilibria
1. Precipitate Equilibrium
Fundamentals of precipitation equilibria.
2. Molar Solubility
Calculations involving molar solubility.
3. Common-Ion Effect
Influence of common ions on solubility.
4. Precipitation and Competing Equilibria
Interactions between precipitation and other equilibria.
5. Drinking Water
Relevance of precipitation equilibria to water quality analysis.
Practice Exercises
Exercises to practice precipitation equilibria concepts.
Part III: Instrumental Methods and Analytical Separations
Chapter 9: Electroanalytical Chemistry
1. Introduction
Basics of electroanalytical methods.
2. Standard Reduction Potentials
Understanding and using standard reduction potentials.
3. Using Half Reactions
Application of half reactions in analysis.
4. Background on Spontaneous Reactions and Equilibrium
Relationship between spontaneous reactions and equilibrium.
5. Reaction Energies, Voltages, and the Nernst Equation
Calculations involving reaction energies and voltages.
6. Electrochemical Cells
Structure and function of electrochemical cells.
7. Potentiometry
Techniques and applications of potentiometry.
8. Ion-Selective Electrodes (ISE)
Use of ion-selective electrodes in analysis.
9. Voltammetry
Principles and applications of voltammetry.
Practice Exercises
Exercises on electroanalytical chemistry.
Chapter 10: Atomic Spectrometry
1. Atomization
Process and significance of atomization in spectrometry.
2. Atomic Absorption Spectrometry (AAS)
Techniques and applications of AAS.
3. Atomic Emission Spectrometry (AES)
Principles of AES.
4. Inductively Coupled Plasma Mass Spectrometry (ICP-MS)
Advanced techniques in mass spectrometry.
5. Other Mass Spectrometer Designs
Overview of various mass spectrometry designs.
Practice Exercises
Exercises on atomic spectrometry techniques.
Chapter 11: Molecular Structure Determination
1. Introduction
Methods for determining molecular structure.
2. Molecular Mass Spectrometry
Principles and applications of molecular mass spectrometry.
3. Fourier-Transform Infrared Spectroscopy (FTIR)
Basics of FTIR.
4. FTIR Instrumentation
Equipment and techniques used in FTIR.
5. Nuclear Magnetic Resonance Spectroscopy (NMR)
Fundamentals of NMR spectroscopy.
6. NMR Instrumentation
Equipment and methods used in NMR analysis.
Practice Exercises
Exercises to practice molecular structure determination.
Chapter 12: Analytical Separations
1. Thin-Layer Chromatography
Techniques and applications of TLC.
2. Chromatogram Terminology
Key terms and concepts in chromatography.
3. Separation Efficiency
Factors affecting separation efficiency.
4. Gas Chromatography (GC)
Principles and practices of GC.
5. Gas Chromatography Mass Spectrometry (GC-MS)
Combined techniques of GC-MS.
6. High Performance Liquid Chromatography (HPLC)
Techniques and applications of HPLC.
7. Electrophoresis
Principles and methods of electrophoresis.
Practice Exercises
Exercises to apply analytical separation techniques.
Index
A comprehensive index to quickly locate topics within the book.
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