Free download Practical Organic Chemistry Including Qualitative Organic Analysis by Arthur I. Vogel Third Edition

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Authors of: Practical Organic Chemistry Including Qualitative Organic Analysis 3rd Edition

Arthur I. Vogel

Table of Contents in Practical Organic Chemistry Including Qualitative Organic Analysis

Preface (Explanation of the book’s purpose, target audience, and changes in the third edition)

Introduction (Importance of practical organic chemistry, basic laboratory techniques and safety)

Part I: Theory of General Technique

• Chapter 1: Distillation (Theory, types of distillation, distillation apparatus)
• Chapter 2: Crystallization (Theory, techniques, solvents, recrystallization)
• Chapter 3: Extraction (Theory, techniques, solvent selection, extraction apparatus)
• Chapter 4: Drying Agents (Types of drying agents, their selection and use)
• Chapter 5: Sublimation (Theory and techniques for sublimation)
• Chapter 6: Chromatography (Basic principles, column chromatography, thin-layer chromatography)

Part II: Qualitative Organic Analysis

• Chapter 7: Detection of the Elements (Tests for C, H, N, S, P, Cl, Br, I)
• Chapter 8: Classification and Preliminary Examination (Separation into acidic, basic, neutral classes, identification of physical properties)
• Chapter 9: Identification of Functional Groups (Tests for alcohols, phenols, aldehydes, ketones, carboxylic acids, esters, amides, amines, etc.)
• Chapter 10: Detection of Specific Organic Compounds (Identification of common organic compounds)

Part III: Preparations

• Chapter 11: Quantitative Determination of Yield (Theory and methods for yield determination)
• Chapter 12: Techniques for Organic Preparations (Heating under reflux, distillation during reaction, drying agents)
• Chapter 13: Hydrocarbons (Preparation of alkanes, alkenes, alkynes, aromatic hydrocarbons)
• Chapter 14: Halogen Derivatives (Preparation of alkyl halides, aryl halides)
• Chapter 15: Alcohols (Preparation of primary, secondary, tertiary alcohols, phenols)
• Chapter 16: Aldehydes and Ketones (Preparation of aldehydes, ketones)
• Chapter 17: Carboxylic Acids (Preparation of carboxylic acids, their derivatives)
• Chapter 18: Esters (Preparation of esters)
• Chapter 19: Amides (Preparation of amides)
• Chapter 20: Amines (Preparation of primary, secondary, tertiary amines)
• Chapter 21: Diazonium Salts and Azo Compounds (Preparation of diazonium salts, azo dyes)
• Chapter 22: Heterocyclic Compounds (Preparation of simple heterocyclic compounds)

Part IV: Quantitative Organic Analysis

• Chapter 23: Determination of Melting Point and Boiling Point
• Chapter 24: Determination of Percentage Composition (Elemental analysis)
• Chapter 25: Determination of Molecular Weight (Methods for molecular weight determination)

Part V: Physical Measurements and Instrumental Techniques

• Chapter 26: Refractometry (Measurement of refractive index)
• Chapter 27: Polarimetry (Measurement of optical rotation)
• Chapter 28: Spectroscopy (Introduction to UV-Vis, IR spectroscopy)

Appendices (Safety data sheets, common laboratory reagents, solubility tables)

Index (Listing of key terms and concepts with page references)

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