Free download Mass Spectrometry of Inorganic Coordination and Organometallic Compounds Tools Techniques Tips By W. Henderson

Tools – Techniques – Tips

Authors of:  Mass Spectrometry of Inorganic Coordination and Organometallic Compounds Tools Techniques Tips By W. Henderson

William Henderson

J Scott McIndoe

Table of Contents in Mass Spectrometry of Inorganic Coordination and Organometallic Compounds Tools Techniques Tips By W. Henderson

The book Mass Spectrometry of Inorganic, Coordination, and Organometallic Compounds: Tools, Techniques, Tips by W. Henderson serves as an in-depth guide to the application of mass spectrometry in analyzing inorganic, coordination, and organometallic compounds.

As mass spectrometry continues to play an increasingly important role in chemical research, this text provides a timely and thorough exploration of how the technique can be used to investigate the structural and compositional nuances of complex compounds in inorganic chemistry. Covering essential principles, it delves into advanced topics such as ionization techniques, instrumentation, and data interpretation specific to this field.

Each section is rich with practical insights, offering readers strategic tips for effectively handling difficult samples and addressing common analytical challenges. Henderson’s work is designed to be accessible to a broad audience, including graduate students, researchers, and industry professionals seeking to deepen their knowledge or acquire new skills in mass spectrometric methods. By emphasizing both theoretical foundations and hands-on applications, this book equips readers to make the most of mass spectrometry in studying the intricate behavior of a wide range of inorganic and organometallic species.

Preface  

List of commonly-used abbreviations  

1 Fundamentals  

1.1 Introduction  

1.2 Inlets  

1.3 Collision-Induced Dissociation  

1.3.1 Bond dissociation energies from CID studies  

1.3.2 Presentation of CID data  

1.4 Detectors  

1.5 Mass Resolution  

1.5.1 Mass accuracy  

1.6 Data Processing  

1.7 Isotopes  

1.7.1 Isotopic abundances of the elements  

1.7.2 Isotope pattern matching  

References  

2 Mass analysers  

2.1 Introduction  

2.2 Sectors  

2.2.1 MS/MS  

2.2.2 Summary  

2.3 Quadrupoles  

2.3.1 MS/MS  

2.3.2 Summary  

2.4 Quadrupole Ion Trap  

2.4.1 MS/MS and MSn  

2.4.2 Summary  

2.5 Time-of-Flight  

2.5.1 Reflectron instruments  

2.5.2 Orthogonal TOF (oa-TOF)  

2.5.3 MS/MS  

2.5.4 Summary  

2.6 Fourier Transform Ion Cyclotron Resonance  

2.6.1 MS/MS  

2.6.2 Summary  

References  

3 Ionisation techniques  

3.1 Introduction  

3.2 Electron Ionisation  

3.2.1 Fragmentation of metal-containing compounds  

3.2.2 Applications  

3.2.3 Summary  

3.3 Chemical Ionisation  

3.3.1 Applications  

3.3.2 Summary  

3.4 Field Ionisation/Field Desorption  

3.4.1 Summary  

3.5 Plasma Desorption  

3.5.1 Applications  

3.5.2 Summary  

3.6 Fast Atom Bombardment / Liquid Secondary Ion Mass Spectrometry  

3.6.1 Matrices  

3.6.2 Ions observed in FAB/LSIMS  

3.6.3 Applications  

3.6.4 Summary  

3.7 Matrix Assisted Laser Desorption Ionisation  

3.7.1 Matrices  

3.7.2 MALDI of air-sensitive samples  

3.7.3 Applications  

3.7.4 Summary  

3.8 Inductively Coupled Plasma Mass Spectrometry  

3.8.1 Applications  

3.8.2 Summary  

3.9 Electrospray Ionisation  

3.9.1 Electrochemistry in the ESI process  

3.9.2 Multiply-charged species  

3.9.3 Nanospray  

3.9.4 ESI MS: Practical considerations  

3.9.5 Applications  

3.9.6 Summary  

References  

4 The ESI MS behaviour of simple inorganic compounds  

4.1 Introduction  

4.2 Simple Metal Salts  

4.2.1 Salts of singly-charged ions M+X  

4.2.2 Salts of multiply-charged ions e.g. M2+(X)2 M3+(X)3 etc.  

4.2.3 Negative-ion ESI mass spectra of metal salts  

4.2.4 ESI MS behaviour of easily-reduced metal ions: copper(II) iron(III) and mercury(II)  

4.3 Polyanions Formed by Main Group Elements  

4.4 Oxoanions Formed by Main Group Elements  

4.5 Borane Anions  

4.6 Fullerenes  

4.7 Inorganic Phosphorus Compounds: Phosphoranes and Cyclophosphazenes  

4.8 Summary  

References  

5 The ESI MS behaviour of coordination complexes  

5.1 Introduction  

5.2 Charged ‘Simple’ Coordination Complexes  

5.2.1 Cationic coordination complexes  

5.2.2 Anionic metal halide complexes  

5.2.3 Highly-charged anionic transition metal complexes – cyanometallate anions  

5.3 (Neutral) Metal Halide Coordination Complexes  

5.4 Metal Complexes of Polydentate Oxygen Donor Ligands: Polyethers Crown Ethers Cryptands and Calixarenes  

5.5 Porphyrins and Metalloporphyrins  

5.6 Metal Alkoxides – Highly Moisture-Sensitive Coordination Compounds  

5.7 α-Diketonate Complexes  

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