Industrial Chemistry Library, High Pressure Process Technology Fundamentals and Applications by A. Bertucco Volume 9
Free Download Industrial Chemistry Library, High Pressure Process Technology Fundamentals and Applications by A. Bertucco Volume 9
Volume 9
Authors of: Industrial Chemistry Library, High Pressure Process Technology Fundamentals and Applications by A. Bertucco Volume 9
A. Bertucco
G. Vetter
Table of Contents in Industrial Chemistry Library, High Pressure Process Technology Fundamentals and Applications by A. Bertucco Volume 9
Preface
Contents
List of Contributors
- Introduction
High pressure definitions and examples in nature
Early historical roots of high-pressure technology
High-pressure technology today – motivations for using high pressure
High-pressure technology today- application survey and examples
- Thermodynamic properties at high-pressure
Introduction
Phase equilibria
Principles of phase equilibria
The Chemical potential and the phase rule of Gibbs
Fugacity and activity
Critical phenomena
Classification of phase equilibria
Fluid phase equilibria
Phase equilibria with the presence of solid phases
Calculation of high-pressure phase equilibria
Bubble point-, dew point- and flash calculations
Equations of state
Cubic equations of state
Non-cubic equations of state
Solubility of solids in Supercritical Fluids
Polymer systems
Glassy polymers
Chemical reaction equilibria
Homogeneous gas reactions
Heterogeneous reactions
Experimental methods
Vapour-Liquid equilibria
Equilibria involving solids
- Kinetic properties at high-pressure
Interesting features at high-pressure
Kinetics of high-pressure reactions
Molecular theory of reaction rate constants
Activation volume
Terms contributing to ΔVR ~
Terms contributing to Δvs #
Evaluation of the activation volume from experimental data
Single homogeneous reactions
Parallel reactions
Reactions in series
Chain reactions
Heterogeneous catalytic reactions
Reactions influenced by mass transport
Prediction of the activation volume
Activation volume as a tool for the elucidation of the reaction mechanism
Change of reaction rate constant with pressure
Problems
Measurement of chemical kinetic data at high pressure
Measurement of reaction rates
Examples
4-Design and construction of high pressure equipment for research and production
High pressure machinery
Requirements and design concepts
Generation of pressure with pumps and compressors
Pumps
Reciprocating displacement pumps
Rotary displacement pumps
Centrifugal pumps
Compressors
Piston compressors
Turbo compressors
Special problems involving high-pressure machinery
Strength of the components
Seals
High-pressure piping equipment
Tubing and fittings
Isolation and control valves
Safety valves and other devices
References of sections 4.1 and 4.2
High-pressure vessels and other components
Calculation of vessels and components
The hollow cylinder under static loading
Strengthening the thick-walled hollow cylinder under static loading
Influence of temperature gradients on design
End pieces side-holes and surface influence
Materials
Typical materials for apparatus and other equipment
Corrosion-resisting materials
H2-attack at elevated temperatures: Nelson diagram
5-Industrial reaction units
6-Separation operations and equipment
7-Safety and control in high pressure plant design and operation
8-Economics of high pressure processes
9-Applications
Chemical reactions in Supercritical Solvents (SCFs)
Enzymatic reactions
Hydrogenation under supercritical single-phase conditions
Supercritical Water Oxidation (SCWO). Application to industrial wastewater treatment
High pressure polymerization with metallocene catalysts
Supercritical Fluid Extraction and Fractionation from Solid Materials
High pressure polymer processing
Precipitation of solids with dense gases
Pharmaceutical processing with supercritical fluids
Treating microorganisms with high pressure
Dry cleaning with liquid carbon dioxide
Dry-cleaning processes
Conventional dry cleaning
Dry cleaning with liquid carbon dioxide
The CO2 dry-cleaning process
Fundamentals
Garments agitation
Machine configurations
Conclusions
Subject Index
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