Heterogeneous Catalysis Fundamentals and Applications By Julian R.H. Ross (informative)
Free download Heterogeneous Catalysis Fundamentals and Applications By Julian R.H. Ross
Authors of: Heterogeneous Catalysis Fundamentals and Applications By Julian R.H. Ross
Julian R.H. Ross
Table of Contents in Heterogeneous Catalysis Fundamentals and Applications By Julian R.H. Ross
Chapter Outline
1.1 Introduction
1.2 Historical Background to Catalysis
1.2.1 Ammonia Decomposition
1.2.2 Catalytic Oxidation
1.2.3 Berzelius and the Concept of Catalysis
1.2.4 The First Industrial Catalytic Processes
1.2.5 Ammonia Synthesis
1.2.6 Steam Reforming of Hydrocarbons
1.2.7 Basic Research on Catalysis
Chapter Outline
2.1 Introduction
2.2 Clean Surfaces
2.3 Langmuir’s Work on Adsorption
2.4 The Langmuir Isotherm
2.5 The Chemisorption of Hydrogen
2.6 The Chemisorption of More Complex Molecules
2.7 Non-homogeneous Surfaces
2.8 Non-equilibrium Adsorption
2.9 The Process of Adsorption
2.10 Some Generalizations on Chemisorption
2.11 Physical Adsorption
2.12 Behaviour of Physical Adsorption Isotherms at Values of P/Po ‡ 0.3
Chapter Outline
3.1 Introduction
3.2 The Catalytic Process
3.2.1 Bimolecular Processes
3.2.2 Unimolecular Processes
3.2.3 Reversibility in Catalytic Processes
3.2.4 Selectivity in Catalytic Processes
3.2.5 Kinetics and Mechanism
3.3 The Catalyst and the Catalytic Site
3.4 Catalysis by Metals
3.4.1 Introductory Remarks
3.4.2 Unsupported Metal Catalysts
3.4.3 Supported Metal Catalysts
3.5 Oxides
3.6 Sulfides
3.7 Conclusions
Chapter Outline
4.1 Importance of Active Surface Area and of Catalyst Structure
4.2 Catalyst Preparation
4.2.1 The Active Surface
4.3 Catalyst Supports
4.3.1 Introductory Remarks
4.3.2 Alumina, Al2O3
4.3.3 Silica, SiO2
4.3.4 SiO2eAl2O3 and Zeolites
4.3.5 Titania, TiO2
4.3.6 Zirconia, ZrO2
4.3.7 Carbon
4.3.8 “Forming” of the Support
4.4 Supported Catalysts
4.4.1 Impregnated Catalysts
4.4.2 Coprecipitated Catalysts
4.4.2.1 Precipitation of single cations
4.4.2.2 Precipitation of several species together: coprecipitation
4.4.2.3 Precipitation and coprecipitation using urea decomposition
4.4.2.4 Decomposition of amino complexes
4.5 Catalyst Characterization
4.5.1 Chemical Composition
4.5.2 Phase Structure
4.5.3 Physical Texture
4.5.4 Catalytic Activity, Selectivity and Stability Under Operating Conditions
Chapter Outline
5.1 Introduction
5.2 Static Reactors
5.3 Stirred and Recirculation Reactors
5.3.1 Stirred Reactors
5.3.2 Recirculation Reactors
5.4 Flow Reactors
5.5 Fluidized Bed Reactors
5.6 Pulse Reactors
5.7 The TAP Reactor
5.8 SSITKA
5.9 “In Situ/Operando” Methods
5.10 Microreactor Methods
5.11 Conclusions
Chapter Outline
6.1 Introduction
6.2 Unimolecular Reaction of Reactant A to Give Products
6.3 Bimolecular Reactions e LangmuireHinshelwood Kinetics
6.4 Bimolecular Reactions e EleyeRideal Kinetics
6.5 The MarseVan Krevelen Mechanism
6.6 Practical Examples of Mechanistic Kinetic Expressions
6.6.1 The Langmuir Equation and the Pressure Function
6.6.2 Ammonia Synthesis
6.6.3 Ethane Hydrogenolysis
6.6.4 Methanation
Chapter Outline
7.1 Introduction
7.2 Catalyst Geometries
7.2.1 Pelleting
7.2.2 Extrusion
7.3 The Importance of Mass Transfer in Catalysis
7.3.1 External Diffusion
7.3.2 Internal Diffusion
7.3.3 Effects of Diffusion Limitations on Selectivity
7.3.4 Effects of Diffusion Limitations on Catalyst Poisoning
7.4 Heat Transfer in Catalysis
7.4.1 Sequential Reactions
7.4.2 Reversible Reactions
7.4.3 Reactors for Exothermic Reversible Reactions
7.4.4 The Chemical Heat Pipe: “The Adam and Eve Process”
Chapter Outline
8.1 Introduction
8.2 Catalysis in the Conversion of Natural Gas
8.2.1 Conversion of Natural gas to Syngas
8.2.2 FischereTropsch Synthesis
8.2.3 Methanol Synthesis and Methanol Reforming
8.2.4 Methanol Conversion to Other Products
8.3 Catalysis in the Conversion of Crude Oil
8.3.1 Crude Oil Distillation and Feedstock Cleaning
8.3.2 Hydrotreating
8.3.2.1. Hydropurification
8.3.3 Isomerization of Light Naphtha
8.3.4 Reforming of Heavy Naphtha
8.3.5 Fluid Catalytic Cracking (FCC)
8.4 Petrochemicals and Industrial Organic Chemistry
8.5 Environmental Catalysis
8.5.1 Selective Reduction of NOx
8.5.2 Automobile Exhaust Catalysts
8.6 Catalysis in Biomass Conversion
8.7 Conclusions
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