The Organic Chem Lab Survival Manual by James W. Zubrick 2nd Edition

Free Download The Organic Chem Lab Survival Manual by James W. Zubrick 2nd Edition
A Student’s Guide to Techniques
2nd Edition
Authors of: The Organic Chem Lab Survival Manual by James W. Zubrick 2nd Edition
James W. Zubrick
Table of Contents in The Organic Chem Lab Survival Manual by James W. Zubrick 2nd Edition
1. Safety First, Last, and Always
Accidents Will Not Happen
2. Keeping A Notebook
A Technique Experiment
Notebook Notes
A Synthesis Experiment
Notebook Notes
3. Interpreting A Handbook
CRC Handbook
Entry: 1-Bromobutane
Entry: Benzoic Acid
Nostalgia
Lange’s
Entry: 1-Bromobutane
Entry: Benzoic Acid
Merck Index
Entry: 1-Bromobutane
Entry: Benzoic Acid
The Aldrich Catalog
Entry: 1-Bromobutane
Entry: Benzoic Acid
Not Clear – Clear?
4. Jointware
Stoppers with Only One Number
Another Episode of Love of Laboratory
Hall of Blunders and Things Not Quite Right
Round-Bottom Flasks
Columns and Condensers
The Adapter With Lots of Names
Forgetting The Glass
Inserting Adapter Upside Down
Inserting Adapter Upside Down Sans Glass
Greasing the Joints
To Grease or Not To Grease
Preparation of the Joints
Into the Grease Pit
Storing Stuff and Sticking Stoppers
Corking a Vessel
The Cork Press
5. Other Interesting Equipment
6. Clean and Dry
Drying Your Glassware When You Don’t Need To
Drying Your Glassware When You Need To
7. Drying Agents
Typical Drying Agents
Using a Drying Agent
Following Directions and Losing Product Anyway
8. On Products
Solid Products
Liquid Products
The Sample Vial
Hold It! Don’t Touch that Vial
9. The Melting Point Experiment
Sample Preparation
Loading the Melting Point Tube
Closing Off Melting Point Tubes
Melting Point Hints
The Mel-Temp Apparatus
Operation of the Mel-Temp Apparatus
The Fisher – Johns Apparatus
Operation of the Fisher – Johns Apparatus
The Thomas – Hoover Apparatus
Operation of the Thomas – Hoover Apparatus
Using the Thiele Tube
Cleaning the Tube
Getting the Sample Ready
Dunking the Melting Point Tube
Heating the Sample
10. Recrystallization
Finding a Good Solvent
General Guidelines for a Recrystallization
Gravity Filtration
The Buchner Funnel and Filter Flask
Just a Note
Activated Charcoal
The Water Aspirator: A Vacuum Source
The Water Trap
Working with a Mixed-Solvent SystemThe Good Part
The Ethanol- Water System
A Mixed-Solvent System-The Bad Part
Salting-Out
World Famous Fan-Folded Fluted Filter Paper
1 1. Extraction and Washing
Never-Ever Land
Starting an Extraction
Dutch Uncle Advice
The Separatory Funnel
The Stopper
The Glass Stopcock
The Teflon Stopcock
The Stem
Washing and Extracting Various Things
How To Extract and Wash What
The Road to Recovery – Back-Extraction
A Sample Extraction
Performing an Extraction or Washing
Extraction Hints
12. And Now – Boiling Stones
13. Sources of Heat
The Steam Bath
The Bunsen Burner
Burner Hints
The Heating Mantle
Proportional Heaters and Stepless Controllers
14. Clamps and Clamping
Clamping a Distillation Setup
15. Distillation
Distillation Notes
Class 1: Simple Distillation
Sources of Heat
The 3-Way Adapter
The Distilling Flask
The Thermometer Adapter
The Ubiquitous Clamp
The Thermometer
The Condenser
The Vacuum Adapter
The Receiving Flask
The Ice Bath
The Distillation Example
The Distillation Mistake
Class 2: Vacuum Distillation
Pressure Measurement
Manometer Hints
Leaks
Pressure and Temperature Corrections
Vacuum Distillation Notes
Class 3: Fractional Distillation
How this Works
Fractional Distillation Notes
Azeotropes
Class 4: Steam Distillation
External Steam Distillation
Internal Steam Distillation
Steam Distillation Notes
16. Reflux
A Dry Reflux
Addition and Reflux
Funnel Fun
How to Set Up
17. Sublimation
18. Chromatography: Some Generalities
19. Thin-Layer Chromatography: TLC
20. Wet-Column Chromatography
21. Dry Column Chromatography
22. Refractometry
23. Instrumentation in the Lab
24. Gas Chromatography
25. HP Liquid Chromatography
26. Infrared Spectroscopy
28. Theory of Distillation
Class 1: Simple Distillation
Clausius & Clapyron
Class 3: Fractional Distillation
Class 4: Steam Distillation
29. Theory of Extraction
File Size: 4.82 MB. Pages: 346 Please read Disclaimer.
Free download The Organic Chem Lab Survival Manual by James W. Zubrick 2nd Edition
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